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Aggregating structure in coal water slurry studied by eDLVO theory and fractal dimension

Qiang LI, Qian WANG, Jian HOU, Jiansheng ZHANG, Yang ZHANG

《能源前沿（英文）》 2023年第17卷第2期页码 306-316 doi: 10.1007/s11708-021-0736-1

摘要： Coal water slurry gasification is a main source of hydrogen in the developing hydrogen economy. Moreover, biomass and waste can be added, making gasification process greener. To expand the application of coal water slurry and gasification process, it is necessary to understand the micro-structure in this large particle suspension system. In this paper, the micro-structure in coal water slurry was studied by extended DLVO (eDLVO) theory and fractal dimension, which is used to explain the mechanism of stability in large particle suspension systems. The interaction between two coal particles was characterized from the interparticle potential and energy barrier based on the eDLVO theory. The rheology and stability between different types of coals are measured and explained by the aggregating structure and fractal dimension in coal water slurry. The results indicated that there would be an aggregating structure in high rank coals, due to the interparticle potential caused by the surface properties, but probably not in low rank coals. This aggregating structure can be described and characterized by fractal dimension. The aggregation of particles is the source of the stability for high rank coals, as the close-packed 3D network structure in large particle suspension can support coal particles from settling down. The results have demonstrated that the combination of the eDLVO theory and rheological measurement is an effective way to investigate the stability of large particle suspension systems.

关键词： coal water slurry extended DLVO (eDLVO) fractal dimension stability

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Development and demonstration plant operation of an opposed multi-burner coal-water slurry gasification

WANG Fuchen, ZHOU Zhijie, DAI Zhenhua, GONG Xin, YU Guangsuo, LIU Haifeng, WANG Yifei, YU Zunhong

《能源前沿（英文）》 2007年第1卷第3期页码 251-258 doi: 10.1007/s11708-007-0035-5

摘要： The features of the opposed multi-burner (OMB) gasification technology, the method and process of the research, and the operation results of a pilot plant and demonstration plants have been introduced. The operation results of the demonstration plants show that when Beisu coal was used as feedstock, the OMB CWS gasification process at Yankuang Cathy Coal Co. Ltd had a higher carbon conversion of 3%, a lower specific oxygen consumption of about 8%, and a lower specific carbon consumption of 2%–3% than that of Texaco CWS gasification at the Lunan Fertilizer Plant. When Shenfu coal was used as feedstock, the OMB CWS gasification process at Hua-lu Heng-sheng Chemical Co. Ltd had a higher carbon conversion of more than 3%, a lower specific oxygen consumption of about 2%, and a lower specific coal consumption of about 8% than that of the Texaco CWS gasification process at Shanghai Coking & Chemical Corporation. The OMB CWS gasification technology is proven by industrial experience to have a high product yield, low oxygen and coal consumption and robust and safe operation.

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砂卵石条件下泥水分离技术研究与应用

王广余,孙善辉,苏清贵

《中国工程科学》 2010年第12卷第12期页码 41-45

摘要：

通过北京铁路北京站至北京西站地下直径线工程泥水处理系统的研究与应用实践经验，总结了城市繁华地段砂卵石条件下大直径盾构泥水分离应用技术，希望对类似工程有借鉴作用。

关键词：泥水盾构泥水分离压滤

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Technology Development and Engineering Practice for Protection and Utilization of Water Resources inCoal Mining in Western China

Da-zhao Gu

《工程管理前沿（英文）》 2016年第3卷第1期页码 59-66 doi: 10.15302/J-FEM-2016010

摘要： Shanxi, Shaanxi, Inner Mongolia, Ningxia, and Gansu (hereafter generally referred as “the Western Area”) are major coal-producing areas in China due to rich coal resources and good mining conditions. However, the Western Area has a serious water shortage. The surface evaporation is huge and a great amount of mine water generated in coal mining is evaporated and lost after discharging to surface. In order to protect and utilize the water resources during large-scale coal mining in the Western Area, Shenhua Group has put forward a technological idea to store mine water in underground mined areas and successfully researched and developed the coal mine underground reservoir technology by solving the technical difficulties of water source prediction, reservoir site selection, reservoir capacity design, dam construction, safety guarantee, water quality control and so on through 20 years of exploration. Now Shenhua Group has successfully established a batch of reservoir in the Shendong Mining Area, obtaining great economic and social benefits. The technology is also extended to other western mining areas, providing an effective path for harmonic mining of coal and water resources in western China.

关键词： Western Mining Area coal mining water resources coal mine underground reservoirs

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Experimental study on slurry-induced fracturing during shield tunneling

Teng WANG, Dajun YUAN, Dalong JIN, Xinggao LI

《结构与土木工程前沿（英文）》 2021年第15卷第2期页码 333-345 doi: 10.1007/s11709-021-0718-8

摘要： Facial support in slurry shield tunneling is provided by slurry pressure to balance the external earth and water pressure. Hydraulic fracturing may occur and cause a significant decrease in the support pressure if the slurry pressure exceeds the threshold of the soil or rock material, resulting in a serious face collapse accident. Preventing the occurrence of hydraulic fracturing in a slurry shield requires investigating the effects of related influencing factors on the hydraulic fracturing pressure and fracture pattern. In this study, a hydraulic fracturing apparatus was developed to test the slurry-induced fracturing of cohesive soil. The effects of different sample parameters and loading conditions, including types of holes, unconfined compressive strength, slurry viscosity, and axial and circumferential loads, on the fracturing pressure and fracture dip were examined. The results indicate that the fracture dip is mainly affected by the deviator stress. The fracturing pressure increases linearly with the increase in the circumferential pressure, but it is almost independent of the axial pressure. The unconfined compressive strength of soil can reflect its ability to resist fracturing failure. The fracturing pressure increases with an increase in the unconfined compressive strength as well as the slurry viscosity. Based on the test results, an empirical approach was proposed to estimate the fracturing pressure of the soil.

关键词： slurry shield tunneling hydraulic fracturing test fracturing pressure fracture dip unconfined compressive strength slurry viscosity

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Modeling of coal swelling induced by water vapor adsorption

Zhejun PAN

《化学科学与工程前沿（英文）》 2012年第6卷第1期页码 94-103 doi: 10.1007/s11705-011-1172-2

摘要： Gas adsorption-induced coal swelling is a well-know phenomenon. Coal swelling or shrinkage by adsorption or desorption of water vapor has not been well understood but has significant implications on gas drainage process for underground coal mining and for primary and enhanced coalbed methane production. Decreased matrix moisture content leads to coal shrinkage and thus the change of cleat porosity and permeability under reservoir conditions. Unlike gas adsorption in coal which usually forms a single layer of adsorbed molecules, water vapor adsorption in the coal micropores forms multilayer of adsorbed molecules. In this work, a model has been developed to describe the coal swelling strain with respect to the amount of moisture intake by the coal matrix. The model extended an energy balance approach for gas adsorption-induced coal swelling to water vapor adsorption-induced coal swelling, assuming that only the first layer of adsorbed molecules of the multilayer adsorption changes the surface energy, which thus causes coal to swell. The model is applied to describe the experimental swelling strain data measured on an Australian coal. The results show good agreement between the model and the experimental data.

关键词： multilayer adsorption vapour pressure coal shrinkage relative humidity permeability

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富水砂卵石地层盾构隧道施工泥浆的研究与应用

邓亨义,徐雪莹,陈明娟

《中国工程科学》 2010年第12卷第12期页码 79-82

摘要：

针对北京站至北京西站地下直径线工程泥水盾构施工，通过对泥浆性能研制的配比试验，提出了砂卵石条件下的最佳泥浆配比，提高并改善了泥浆的成形质量与速度，确保了环境要求。对类似工程有一定的借鉴作用。

关键词：泥水盾构砂卵石地层泥浆配合比

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富水砂卵石地层大直径泥水盾构施工地表沉降规律

赵宝华,胡曦波,张兵,李文俊

《中国工程科学》 2010年第12卷第12期页码 94-97

摘要：

北京地下直径线工程位于富水砂卵石地层中，穿越诸多建（构）筑物。通过实际监测结果分析，总结掘进参数与地表沉降之间的规律及隧道周围重要建筑物的变形规律，经与类似工程比较后发现本工程在变形控制上有很大的成效。

关键词：富水砂卵石大直径泥水盾构沉降规律

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富水砂卵石地层中大直径泥水盾构同步注浆技术

张长强,翟志国,陈明娟,金仲祥

《中国工程科学》 2010年第12卷第12期页码 75-78

摘要：

通过统计分析盾构掘进相关技术资料，综合考虑富水砂卵石地层中泥水盾构掘进参数、泥浆参数、盾构姿态、地层变形机理等信息，确定泥水盾构在砂卵石地层中掘进时，同步注浆主要技术参数间的经验公式，指导类似工程施工。

关键词：砂卵石地层泥水盾构同步注浆施工技术

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大埋深富水砂卵石地层泥水盾构带压换刀及动火焊接技术

程明亮,何峰,吕传田

《中国工程科学》 2010年第12卷第12期页码 46-50

摘要：

通过北京铁路地下直径线工程盾构施工实践经验，总结了大埋深富水砂卵石地层泥水盾构施工中带压换刀技术以及特殊情况下的带压动火焊接技术。带压换刀的技术主要有两个方面:一是选择合理换刀地点及进舱工作压力，保证掌子面土体的稳定；二是进行开挖舱高浓度泥浆的置换和中盾高浓度泥浆的注入，有效地防止了气体的逃逸。在施工中成功实现了带压进舱250余次，工作压力从0.9 bar (1 bar=100 kPa)增加到2.8 bar，未发生任何安全事故。

关键词：泥水盾构砂卵石地层富水地层带压换刀焊接

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Copper fractal growth during recycling from waste printed circuit boards by slurry electrolysis

《环境科学与工程前沿（英文）》 2021年第15卷第6期 doi: 10.1007/s11783-021-1405-7

摘要：

• Copper fractal growth was observed during WPCBs recycling by slurry electrolysis.

关键词： Dendritic copper Fractal growth WPCBs Slurry electrolysis

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Kinetic study of hydrodesulfurization of coker gas oil in a slurry reactor

Haiding XIANG, Tiefeng WANG

《化学科学与工程前沿（英文）》 2013年第7卷第2期页码 139-144 doi: 10.1007/s11705-013-1323-8

摘要： Coker gas oil (CGO) is a poor-quality feedstock for fluidized bed catalytic cracking (FCC) or hydrocracking. The pretreatment of CGO, especially hydrotreating, can significantly improve the product quality and protect the catalyst. In this work, we studied the hydrodesulfurization (HDS) of CGO in a slurry reactor. All the experiments were carried out in an autoclave using a NiMo/Al O catalyst at reaction temperature 340°C–400°C, pressure 6–10 MPa, and stirring speed 800 r·min , with hydrogen-to-oil ratio in the range of 500–1500. The effects of the operating parameters on the desulfurization ratio were investigated and discussed. A macro reaction kinetic model was established for the HDS of CGO in the slurry reactor.

关键词： coker gas oil hydrodesulfurization slurry reactor reaction kinetic model

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Experimental study on the stratum applicability and mechanisms of bubble–slurry for earth pressure balance

《结构与土木工程前沿（英文）》页码 1387-1399 doi: 10.1007/s11709-023-0005-y

摘要： Soil conditioning is essential for addressing the stratum applicability problem of earth pressure balance (EPB) shields. Under high water pressures, EPB shields spew water and soil when excavating coarse-grained strata. Typically, foam combined with polymers and slurry is used to solve spewing. However, in current techniques, slurry, foam, and the other agents are mixed with soil separately, their synergistic effect is seldom realized. In this study, an anionic surfactant was used to foam in bentonite slurry to form bubble–slurry to maximize the synergy between bubbles and slurry. The slump, volume stability, and permeability test of bubble–slurry-conditioned sand was conducted to examine the conditioning effect, and the stratum applicability of bubble–slurry was determined from the perspective of permeability. It was found that the conditioning effect of bubble–slurry in coarse gravel soil was excellent and could expand the applicability of EPB shields. The main stabilization mechanism of bubble–slurry is that bentonite particles provide a space barrier for bubbles. And three seepage modes of bubble–slurry-conditioned sand were innovatively defined, and the occurrence conditions of the three seepage modes were analyzed according to the permeability coefficient of sand, initial dynamic shear force of bubble–slurry, and hydraulic gradient.

关键词： EPB shield bubble–slurry soil conditioning stability permeability

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Hydrogen production from co-gasification of coal and biomass in supercritical water by continuous flow

YAN Qiuhui, GUO Liejin, LIANG Xing, ZHANG Ximin

《能源前沿（英文）》 2007年第1卷第3期页码 327-330 doi: 10.1007/s11708-007-0048-0

摘要： Hydrogen is a clean energy carrier. Converting abundant coal sources and green biomass energy into hydrogen effectively and without any pollution promotes environmental protection. The co-gasification performance of coal and a model compound of biomass, carboxymethylcellulose (CMC) in supercritical water (SCW), were investigated experimentally. The influences of temperature, pressure and concentration on hydrogen production from co-gasification of coal and CMC in SCW under the given conditions (20–25 MPa, 650vH, 15–30 s) are discussed in detail. The experimental results show that H, CO and CH are the main gas products, and the molar fraction of hydrogen reaches in excess of 60%. The higher pressure and higher CMC content facilitate hydrogen production; production is decreased remarkably given a longer residence time.

关键词： carboxymethylcellulose temperature co-gasification performance Hydrogen residence

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Study on direct alcohol/ether fuel synthesis process in bubble column slurry reactor

Zhen CHEN, Haitao ZHANG, Weiyong YING, Dingye FANG

《化学科学与工程前沿（英文）》 2010年第4卷第4期页码 461-471 doi: 10.1007/s11705-010-0517-6

摘要： The recent studies of direct alcohol/ether synthesis process in slurry reactors were reviewed, and the research work in our laboratory was carried out in this paper. a global kinetics model for direct dimethyl ether (DME) synthesis from syngas over a novel Cu-Zn-Al-Zr slurry catalyst was established according to the total of 25 experimental data, and a steady-state one-dimensional mathematical model was further developed in bubble column slurry reactor (BCSR), which was assumed that the bubble phase was plug flow, and the liquid phase was fully mixed flow. The numerical simulations of reactor design of 100000 t/a dimethyl ether pilot plant indicate that higher pressure and lower temperature were favorable to the increase of CO conversion, selectivity of dimethyl ether, product yield and height of slurry bed. The optimal operating conditions for DME synthesis process were obtained: reaction temperature at 240°C, reactor pressure at 5 MPa and reactor diameter of 2.5 m.

关键词： syngas alcohol/ether fuel slurry catalyst bubble column slurry reactor global kinetics mathematical model